快速微量馏程仪-PMD100-工作原理.pptx

PMD100 ISL1ISL MICRO DISTILLATION PMD100PMD100 ISL2Presentation summary PMD operation principleDesignAdvanced featuresApplication Sample dataPMD100 ISL3Operational principalPMD100 ISL4Physical distillationMeasures and records vapors&liquid temperatures,further monitoring in-flask pressure as sample gradually distills under atmospheric pressureFIG.A1.1 Schematic of MicroDist ApparatusPMD100 ISL5Operation principle flow chartHow does it work?Physical distillation10 ml of liquid specimenAcquisition anddata record(TL,Tv,P,t)6 to 8 min“True”PMD curve Tvap=()Conversion to D86-complaintformat1 to 2 min+Results reportingin C or FBarometriccorrection=10 min maxPMD100 ISL6What is going inside?IBPFBPPMD100 ISL7D86 distillation curve calculated and reportedTemperature C versus Volume%Temperature C versus Volume%PMD100 ISL8Result reporting lComplete distillation data on the local displaylDistillation curve can be printed with a graphic printerlStandard or customized report on the display or a printerlResults can be automatically compared with specificationsPMD100 ISL9Result printoutDate/time of print PMD 100 dataSample IDDate/time of testResultsStep=default(1%,5%,10%steps choice)Productparameters26/08/2001 18:58 ISL PMD 100Product:7 FUEL ROUGE No:003 Op :LG 15/02/2001 10:09 AtmPrs:102.8kPaEvaporated results with barom.corr.IBP 163.7 10%181.9 20%195.3 30%212.2 40%229.1 50%250.6 60%270.6 70%291.9 80%313.5 90%336.1 FBP 361.6 97.1%Product:7 FUEL ROUGE Start Tmp 30C Bar.Cor:NO Spec%(Tmp min max):Not used Spec T(Typical Tmp):Not used 5%172.2 95%354.2Software V1.4/1.3 S/N:572PMD100 ISL10DesignPMD100 ISL11Micro Distillation PMD100 lEasy to use and FastlPhysical distillation testlCompact and IndependentlRobust and SafeFriendly for untrained people without exposure to laboratory equipment !PMD100 ISL12Easy to use1234Charge 10ml of sample into flask Place measurement head onto flask and load the flask into the test portPress the“Start”key to begin the testNo programs or heating power selection necessaryThe test starts immediatelyDoes not require any apparatus conditioning before a test or any cleaning following a testComplete distillation data on the display in less than 10 minutesResults can be automatically compared with specificationsASTM D86 distillation curve printed with a graphic printerStandard or customized reporting on the printerPC software is available for data collection and networking up to 20 PMD100PMD100 ISL13High throughputC Complete result report in Automatic and time recorded calibrations Simple calibration by distillation of two pure compounds Conventional way by using liquid bath is available Ability to print out calibration reports Calibration frequency taggingPMD100 ISL18Tactile and solventproof keypadLarge LCD screen600mm(24in.)250mm(10in.)The only portable distillation instrument on the marketlWeight:17 kg(37 lbs.)l100-250V ACl250W power consumptionPMD100 ISL19No option:all is includedRS232C and RS485 interfaces100./.240V50-60 HzPrinter connectionPMD100 ISL20Advanced usePMD100 ISL21Pass/fail operationlBy setting product name at start of a test user can associate it with defined specificationl At the end of the run a system message automatically warns the operator if obtained result fall outside defined specificationslIn-spec/out-spec quality statement with detailslCustomized displayed or printed reportPMD100 ISL22Product list Select a product name in pre-programmed listC up to 40 names could be memorizedC each product can be linked to defined spec Product:Unit:COp:ProductOper.Samp IDStartnowSamp ID:ProductPg UpOtherSelect a productPg DwnOk1:Default2:Gasoline3:Unleaded4:Diesel5:Jet A-16:Reformat7:Light nafta8:Heavy nafta9:10:PMD100 ISL23Spec control Obtained result instantaneously compared to product specF Up to 80 specifications can be memorizedC In spec/Out spec warning message with detailsCTwo types of spec can be applied for one product163,9174,4182,7196,3Spec(Tmp mini max)3:FuelOn/OffSelectV%Res C Spec Tmin C Tmax CIBP51020OKOk160170183190170176185195UnitSpec TSpec%Evaporated without barometric correct.IBP5%10%20%30%EP40%50%60%70%80%232,9 C255,9 C278,7 C300,4 C322,8 C346,4 C359,2 C90%95%365,3163,9 C174,4 C182,7 C196,3 C214,5 CDETAILS DISPLAYSPECIFICATIONSDISPLAYSPEC.ONBar.CorOut of Spec%R 97,1%PMD100 ISL24SpecsProductSpecTRun environment printing/displayingSpec%Result Spec.Select a result spec.(Tmp min max)PrintPg UpDetails1:2:3:FUEL4:KERO CARP5:Gasoil H6:7:8:9:10:CCCCCCCCCCSelect a result spec.(Typical Tmp)PrintPg UpDetails1:2:3:FUEL4:KERO CARP5:Gasoil H6:7:8:9:10:CCCCCCCCCCTwo kinds of specifications can be applied:FPercent of evaporation for given temperatureFTypical temperatures per volumePMD100 ISL25ApplicationPMD100 ISL26Micro Distillation PMD100 lProducts application:Fuels group 1 to 4 according ASTM D86 classification:gasoline,jet fuels,diesel fuelsLight and middle distillates with boiling range greater than 10degC(20degF)lResults typical with those of ASTM D86 or its analogs with better repeatabilityPMD100 ISL27PMD100 Market placeThe instrument proves ideal for applications where:standard laboratory instrumentation cannot be applied or is restricted due to:insufficient response time,small sample volume availability,dimension or weight limitations,or untrained staff.October 2001,World Refining magazine:“Using only 10mLs and requiring less than 10 minutes for analysis,ISLs new MicroDist technology significantly increases test productivity supplying quick,reliable results in correlation to ASTM D 86.”PMD100 ISL28 PMD100 application:Rugged,fully independent,stand-alone unit enables installation at locations ideal to workflow and operation by personal with no analytical experience:lMobile/Field application Military,Customs,Quality inspection,.Can be installed in the mobile laboratoryFor product identification and fast quality evaluationlPipelines&TerminalsFast check of product boiling range in conformance with certificate-Contamination monitoringlDistribution Product quality screening on service stationslResearch-Fast product evaluation with small sample volumelRefinery-At-line or laboratory application for fast response analysis on refining process quality follow-upPMD100 ISL29lRefining Process controlPMD100 ISL30Sample dataPMD100 ISL31Sample Data:GasolinePMD100 ISL32Sample Data:20 CutPMD100 ISL33Sample Data:Jet FuelPMD100 ISL34Sample Data:Diesel FuelPMD100 ISL35ISL MICRO DISTILLATION PMD100