梅特勒4000TOC仪器使用手册.pdf

Total Organic Carbon Measurement SystemOperation Manual 4000TOC SensorM300 TOC Transmitter4000TOC Sensor M300 TOC Transmitter 58 130 196 Rev B4000TOC Sensor 2 05/14 Mettler-Toledo Thornton 4000TOC SensorPrinted in USA 4000TOC Sensor 3 05/14 Mettler-Toledo Thornton 4000TOC SensorPrinted in USA Operation Manual 4000TOC SensorM300 TOC Transmitter4000TOC Sensor 4 05/14 Mettler-Toledo Thornton 4000TOC SensorPrinted in USA 4000TOC Sensor 5 05/14 Mettler-Toledo Thornton 4000TOC SensorPrinted in USA Content1 Introduction _ 92 Safety instructions_102.1Definitionofequipmentanddocumentationsymbolsanddesignations _102.2Correctdisposaloftheunit _113 Unit overview_123.1 Overview,4000TOC Sensor _123.1.1SensorDetails _123.1.2HighPressureApplications _133.1.3PotentialCondensationApplications _133.1.4HighTemperatureApplications _133.2 Overview,M300 TOC _133.2.1 1/4DIN _133.2.2 1/2DIN _143.3Control/NavigationKeys _143.3.1MenuStructure _143.3.2Navigationkeys _153.3.2.1 Navigatingthemenutree _153.3.2.2 Escape _153.3.2.3 Enter _153.3.2.4 Menu _153.3.2.5 Calibrationmode _153.3.2.6 Infomode _153.3.3Navigationofdataentryfields _153.3.4Entryofdatavalues,selectionofdataentryoptions _153.3.5NavigationwithuinDisplay _163.3.6”Savechanges”dialog _163.3.7SecurityPasswords _163.4Display _164 M300 TOC Installation instruction _174.1UnpackingandinspectionoftheM300TOC _174.1.1Panelcutoutdimensionalinformation 1/4DINmodels _174.1.2Installationprocedure1/4DINmodels _184.1.3Panelcutoutdimensionalinformation 1/2DINmodels _194.1.4Installationprocedure1/2DINmodels _204.1.5Assembly1/2DINversion _204.1.61/2DINversionDimensiondrawings _214.1.71/2DINversionPipemounting _214.1.81/4DINversionDimensiondrawings _224.2Connectionofpowersupply _234.2.11/4DINhousing(panelmount)_234.2.21/2DINhousing(wallmount)_244.3ConnectorPINdefinition _244.3.1TB1andTB2for1/2DINand1/4DINversions _254.3.2TB3for1/2DINand1/4DINversions _254.4ConnectionofTOCSensor _255 4000TOC Installation Instructions _265.1Unpackingandinspectionofthe4000TOC _265.2Installationofthe4000TOC _265.3SampleTubingConnections _275.4SampleConditioningCoil _285.5ACPowerConnection _295.6SensorConnection _306 Placing transmitter in,or out,of service _316.1Placingtransmitterinservice _316.2Placingtransmitteroutofservice _317 4000TOC Sensor Operation _327.1InitialStartup _327.2SettingSampleFlowRate _327.3StartTOCMeasurement _337.4NormalOperation _337.5SystemSuitabilityTesting _344000TOC Sensor 6 05/14 Mettler-Toledo Thornton 4000TOC SensorPrinted in USA 7.6Calibration _347.6.1TOCCalibrationMethods _348 Quick Setup _369 Sensor Calibration _379.1EnterCalibrationMode _3710 Configuration _3810.1 EnterConfigurationMode _3810.2 Measurement _3810.2.1 ChannelSetup _3810.2.2 Conductivity/ResistivityTemperatureCompensation _3910.2.3 SetAveraging _3910.3 TOCSetup _4010.3.1 TOCGeneralParameters _4010.3.2 LampControl _4110.3.3 Autobalance _4110.4 AnalogOutputs _4210.5 _Setpoints _4310.6 Alarm _4610.7 Display _4710.7.1 Measurement _4710.7.2 Resolution _4810.7.3 Backlight _4810.7.4 Name _4810.8 HoldAnalogOutputs _4911 System _5011.1 SetLanguage _5011.2 USB _5011.3 Passwords _5111.3.1 ChangingPasswords _5111.3.2 ConfiguringMenuAccessforOperator _5111.4 Set/ClearLockout _5111.5 Reset _5211.5.1 ResetSystem _5211.5.2 ResetAnalogCalibration _5211.5.3 ResetSensorCalibrationDatatoFactorySettings _5311.5.4 ResetCalibrationDataofSensorElectronicstoFactorySettings _5312 4000TOC Sensor Service Requirements _5412.1 UVLampReplacement _5412.2 HighCapacityInletFilterReplacement _5513 M300 TOC Service _5613.1 EnterServiceMenu _5613.2 Diagnostics _5613.2.1 Model/SoftwareRevision _5613.2.2 DigitalInput _5713.2.3 Display _5713.2.4 Keypad _5713.2.5 Memory _5713.2.6 SetRelay _5813.2.7 ReadRelays _5813.2.8 SetAnalogOutputs _5813.2.9 ReadAnalogOutputs _5813.3 Calibrate _5913.3.1 VerifyConductivityElectronics _5913.3.2 CalibrateAnalog _5913.3.3 CalibrateUnlock _6013.4 TechService _6014 Info _6114.1 InfoMenu _6114.2 Messages _6114.3 CalibrationData _6114.4 Model/SoftwareRevision _6214.5 TOCSensorInfo _6215 Maintenance _6315.1 ForTechnicalSupport _6315.2 FrontPanelCleaning _634000TOC Sensor 7 05/14 Mettler-Toledo Thornton 4000TOC SensorPrinted in USA 16 Troubleshooting the M300 TOC Transmitter _6416.1 ChangingtheFuse _6416.2 Warning-andAlarmindicationonthedisplay _6516.2.1 Warningindication _6516.2.2 Alarmindication _6517 Troubleshooting the 4000TOC Sensor _6617.1 BasicTroublshooting _6617.2 FaultandErrorMessages _6618 Accessories and Spare Parts _6818.1 M300 TOC Transmitter _6818.2 4000TOC Sensor _6818.2.1 4000TOCSensorSpareParts _6818.2.2 4000TOCSensorConsumableItems _694000TOC Sensor 8 05/14 Mettler-Toledo Thornton 4000TOC SensorPrinted in USA 4000TOC Sensor 9 05/14 Mettler-Toledo Thornton 4000TOC SensorPrinted in USA 1 IntroductionStatementofintendeduseThe4000TOCsensorisaTotalOrganicCarbonsensordesignedtomeasuretheconcentrationoforganicsubstancesinpureandultrapurewaterapplications.TheM300TOCisasinglechanneltransmitterwithalargefourlinebacklitLiquidCrystalDisplaywhichconveysmeasuringandsetupinformationforthe4000TOCsensor.Whenusedincombination,the4000TOCsensorandM300TOCtransmitter,formaTOCmea-surementsystemwhichprovidesthedesignflexibilityforfullintegrationintowatersystems.Theseparatecomponentsallowforclosepositioningofthesensortothesamplepointforfastestre-sponse,whileallowingintegrationofthetransmitterintothecontrolsystem.Thismanualappliestothe4000TOCsensor,andM300TOCtransmitter:4000TOCDesignationOrderno.4000TOCSensor,110VAC,50/60Hz 580360214000TOCSensor,220VAC,50/60Hz 58036022M300 TOCDesignationOrderno.M300 TOC 1/4DIN 58 006 302M300 TOC 1/2DIN 58 006 312Throughoutthisman ual,thetermsM300andM300TOCareused.Withinthecontextofthisdocument,bothtermsshouldbetakentorefertotheM300TOCtransmitter.Theprintscreenimagesinthismanualhaveageneralexplainingcharacterandcandifferfromtherealdisplayinyourtransmitter.Thisdescriptioncorrespondstothefirmwarerelease,version1.0oftheM300TOCtransmitter.Changesaretakingplaceconstantly,withoutpriornotification4000TOC Sensor 10 05/14 Mettler-Toledo Thornton 4000TOC SensorPrinted in USA 2 Safety instructionsThismanualincludessafetyinformationwiththefollowingdesignationsandformats.2.1 Definitionofequipmentanddocumentationsymbolsand designationsa WARNING:POTENTIALFORPERSONALINJURY.a CAUTION:possibleinstrumentdamageormalfunction.h NOTE:Importantoperatinginformation.a On the transmitter or in this manual text indicates:Cautionand/orotherpossiblehazardin-cludingriskofelectricshock(refertoaccompanyingdocuments).Thefollowingisalistofgeneralsafetyinstructionsandwarnings.Failuretoadheretothesein-structionscanresultindamagetotheequipmentand/orpersonalinjurytotheoperator.TheM300Transmittershouldbeinstalledandoperatedonlybypersonnelfamiliarwith thetransmitterandwhoarequalifiedforsuchwork.TheM300Transmittermustonlybeoperatedunderthespecifiedoperatingconditions(seesection19).RepairoftheM300Transmittermustbeperformedbyauthorized,trainedpersonnelonly.Withtheexceptionofroutinemaintenance,cleaningproceduresorfusereplacement,asdescribedinthismanual,theM300Transmittermustnotbetamperedwithoralteredin anymanner.Mettler-Toledoacceptsnoresponsibilityfordamagecausedbyunauthorizedmodifica-tions tothetransmitter.Followallwarnings,cautions,andinstructionsindicatedonandsuppliedwiththisprod-uct.Installequipmentasspecifiedinthisinstructionmanual.Followappropriatelocalandnationalcodes.Protectivecoversmustbeinplaceatalltimesduringnormaloperation.Ifthisequipmentisusedinamannernotspecifiedbythemanufacturer,theprotectionprovidedbyitagainsthazardsmaybeimpaired.WARNINGS:Installationofcableconnectionsandservicingofthisproductrequireaccesstoshockhazardvoltagelevels.Mainpowerandrelaycontactswiredtoseparatepowersourcemustbedisconnectedbe-foreservicing.SwitchorcircuitbreakershallbeincloseproximitytotheequipmentandwithineasyreachoftheOPERATOR;itshallbemarkedasthedisconnectingdevicefortheequip-ment.Mainpowermustemployaswitchorcircuitbreakerasthedisconnectingdevicefortheequipment.a 4000TOC Sensor 11 05/14 Mettler-Toledo Thornton 4000TOC SensorPrinted in USA ElectricalinstallationmustbeinaccordancewiththeNationalElectricalCodeand/oranyotherapplicablenationalorlocalcodes.Safetyandperformancerequirethatthisinstrumentbyconnectedandproperlygroundedthroughathree-wirepowersource.h NOTE!RELAY CONTROL ACTION:theM300transmitterrelayswillalwaysde-energizeonlossofpower,equivalenttonormalstate,regardlessofrelaystatesettingforpoweredoperation.Config-ureanycontrolsystemusingtheserelayswithfail-safelogicaccordingly.h NOTE!PROCESS UPSETS:Becauseprocessandsafetyconditionsmaydependonconsistentoperationofthistransmitter,provideappropriatemeanstomaintainoperationduringsensorcleaning,replacementorsensororinstrumentcalibration.h NOTE:Thisisa4-wire-productwithanactive420mAanalogoutput.PleasedonotsupplytoPin1Pin6ofTB2.2.2 Correct disposal of the unit Whenthetransmitterisfinallyremovedfromservice,observealllocalenvironmentalregulationsforproperdisposal.4000TOC Sensor 12 05/14 Mettler-Toledo Thornton 4000TOC SensorPrinted in USA 3 Unit overviewM300modelsareavailableinbotha1/4DINand1/2DINcasesize.The1/4DINisapanel-mountonlydesignandthe1/2DINmodelsprovideanintegralIP65housingforwall-,orpipe-mount.3.1 Overview,4000TOC Sensor3.1.1 Sensor DetailsThe4000TOCSensorisaTotalOrganicCarbonsensordesignedforusewiththeM300TOCtransmitter.TheM300TOCwillautomaticallyidentifythe4000TOCSensorwhenitisconnect-ed,andallfactorycalibrationdataisautomaticallyreadandusedforoperationandindication.The4000TOCSensorandM300TOCtransmitterareconfiguredwithfactorydefaultsettingstominimizemeasurementsetuptime.Thesedefaultsettingsallowforsensoroperationwithmini-malkeystrokes.The4000TOCSensorhasmorefeaturesthanothersensorsandmayrequireadditionalconfigurationdependantupontheoperationalsetup.Oncetheseparametersareset,theTOCsensorwillfunctionautomatically,andwillrequireuserinterfaceonlyforperiodicser-viceandmaintenance.Measurementsavailablefromthe4000TOCSensorincludeTOC,Con-ductivity/Resistivity(compensatedanduncompensated)andTemperature.The4000TOCSensorisdesignedwithfourlocalLEDindicatorsandaUVLampcontrolkeyonthefrontpanel,asshownintheillustrationbelow.TheLEDsaredesignedtoprovidelocalindi-cationofsensorstatus.TheoperationoftheLEDsissynchronizedwiththeM300TOCdisplaystatusmessagesthatappearinthe6-digitmeasurementnamelocation.FunctionColorOperationFaultRedFlashesduringFaultcondition,sensoroperationstoppedErrorAmberIlluminatesduringErrorcondition,sensorremainsoperationalSensorStatusGreenIlluminateswheneverACPowerisonandtheM300TOCisconnectedtothesensorUVLampOnGreenIlluminateswhenevertheUVLampisonTheUVLampcontrolkeyisdesignedtoprovidealocalOn/OffcontrolfortheUVlamptoallowforquicklampchange-outandassisttheoperatorduringtroubleshooting,ifnecessary.NOTE:IftheUVLampKeyispressedtoturntheUVLampoff,theUVLampcannotbeturnedonfromtheM300TOC,itcanonlybeturnedonbypressingthesensorkeyagain.h4000TOC Sensor 13 05/14 Mettler-Toledo Thornton 4000TOC SensorPrinted in USA Thefrontcoverofthesensorishingedontheleftside.Locatedatthetopandbottomrightcor-nersofthesensorenclosurearetwotriangle-shapeddoorfasteners.Theinstallationkitprovid-edwiththeSensorincludesthespecialtoolneededtoloosenthesefastenersandopenthefrontdoortotheenclosure.Periodicaccesswillberequiredtoperformroutineserviceandmainte-nance.AdditionalfrontcovertoolsareavailablefromMettler-ToledoThornton,Inc.SeeSection18forpartnumbersanddescriptions.3.1.2 High Pressure ApplicationsForinstallationswithprocesspressureabove85psig(5.9bar),theHighPressureRegulator(p/n58091552)isrequired(seesection5.3).InstallationinstructionsaresuppliedwiththeHighPressureRegulator.3.1.3 Potential Condensation Applications Certainambientandprocesstemperaturesmaycausecondensationtooccurinsidethe4000TOCSensor.TheMettler-ToledoThorntonSampleConditioningCoilprovidedwiththesensorinstallationkitisdesignedtoreducecondensationconditionsbyallowingthesampletemperaturetopartiallyequalizewiththeambienttemperature.3.1.4 High Temperature ApplicationsForwatertemperaturesabove70C(158F),theSampleConditioningCoil(p/n58091511)isrequired.Inhighpressureapplications,theHighPressureRegulator(p/n58091552)mustbeinstalleddownstreamoftheSampleConditioningCoil.3.2 Overview,M300 TOC3.2.1 1/4DIN45678 4.011024.01102EnterInfoMETTLER TOLEDOESCMenuCalM3001231:HardPolycarbonatecase5:USBInterfacePort2:FiveTactile-FeedbackNavigationKeys6:RelayOutputTerminals3:Four-lineLCDDisplay7:AnalogOutput/DigitalInputTerminals4:PowerSupplyTerminals8:SensorInputTerminals4000TOC Sensor 14 05/14 Mettler-Toledo Thornton 4000TOC SensorPrinted in USA 3.2.2 1/2DIN5.901505.90150EnterInfoCalMenuM300123ESC 456781:HardPolycarbonatecase5:USBInterfacePort2:FiveTactile-FeedbackNavigationKeys6:RelayOutputTerminals3:Four-lineLCDDisplay7:AnalogOutput/DigitalInputTerminals4:PowerSupplyTerminals8:SensorInputTerminals3.3 Control/Navigation Keys3.3.1 Menu StructureBelowisthestructureoftheM300menutree:MeasurementMode M300CalMenuInfoQuick SetupConfigureSystemServiceMessagesTOC Sensor InfoMeasurementAnalog OutputsSet PointsAlarm/CleanDisplaySet LanguageUSBPasswordsSet/Clear LockoutResetCalibrateTech ServiceDiagnosticsHold OutputsCalibration DataModel/SoftwareRevisionChannel SetupAnalog OutputsSet PointsSet FlowSet FlowUV Lamp4000TOC Sensor 15 05/14 Mettler-Toledo Thornton 4000TOC SensorPrinted in USA 3.3.2 Navigation keysMenuCalInfoEnterESC3.3.2.1 Navigating the menu treeEnterthedesiredmainMenubranchwiththe or keys.Usetheandkeystonavi-gatethroughtheselectedMenubranch.h NOTE:Inordertobackuponemenupage,withoutescapingtothemeasurementmode,movethecursorundertheUPArrowcharacter(u)atthebottomrightofthedisplayscreenandpressEnter.3.3.2.2 EscapePresstheandkeysimultaneously(escape)toreturntotheMeasurementmode.3.3.2.3 EnterUsetheekeytoconfirmactionorselections.3.3.2.4 MenuPressthekeytoaccessthemainMenu.3.3.2.5 Calibration modePressthekeytoenterCalibrationMode.3.3.2.6 Info modePressthekeytoenterInfoMode3.3.3 NavigationofdataentryfieldsUsethekeytonavigateforwardorthe keytonavigatebackwardswithinthechangeabledataentryfieldsofthedisplay.3.3.4 Entry of data values,selection of data entry options4000TOC Sensor 16 05/14 Mettler-Toledo Thornton 4000TOC SensorPrinted in USA Usethekeytoincreaseorthekeytodecreaseadigit.Usethesamekeystonavigatewith-inaselectionofvaluesoroptionsofadataentryfield.h NOTE:Somescreensrequireconfiguringmultiplevaluesviathesamedatafield(ex:configuringmultiplesetpoints).Besuretousethe or keytoreturntotheprimaryfieldandthe or keytotogglebetweenallconfigurationoptionsbeforeenteringtothenextdisplayscreen.3.3.5 Navigation with u in DisplayIfauisdisplayedonthebottomrighthandcornerofthedisplay,youcanusetheorthe keytonavigatetoit.IfyouclickENTERyouwillnavigatebackwardsthroughthemenu(gobackonescreen).Thiscanbeaveryusefuloptiontomovebackupthemenutreewithouthavingtoexitintothemeasuringmodeandre-enterthemenu.3.3.6”Save changes”dialogThreeoptionsarepossibleforthe”Savechanges”dialog:Yes&Exit(Savechangesandexittomeasuringmode),”Yes&u”(Savechangesandgobackonescreen)and”No&Exit”(Dontsavechangesandexittomeasuringmode).The